Samsung RT34M Instrukcja Użytkownika Pobierz pdf (Strona 8)

Dushyant Patel List of Tables

S.K.P.C.P.E.R., Kherva I M .Pharm. Thesis

List of Tables

Table

No.

Title

Page

No.

2.1

Official analytical method

2.2 Reported analytical methods 8

4.1

Different scan mode (MS & MS/MS)

4.2 Reference/working standards 31

4.3 Apparatus 31

4.4 Instrumentation 31

4.5 Reagents and chemicals 31

4.6 Preparation of calibration standard and quality control spiking solutions 34

4.7

Preparation of calibration standards and quality control samples in

biological matrix with respect to 5 % spiking.

4.8 Tuning parameters for GBP & LEV (IS) 36

4.9 Method development trials 37

4.10 Selection of calibration standard 43

4.11 Specificity and selectivity of blank human plasma for GBP & LEV 53

4.12 Sensitivity (LLOQ of GBP) 53

4.13 Summary of calibration curve parameters of GBP 54

4.14

Back calculated concentration of calibration standards from calibration

curve of GBP

4.15 Within-batch or intra-batch accuracy and precision of GBP 55

4.16 Between-batch or inter- batch accuracy and precision of GBP 56

4.17 Recovery of GBP 58

4.18 Variability across QC levels of GBP 58

4.19 Recovery of internal standard (LEV) 59

4.20 Dilution integrity of GBP 59

4.21 Matrix effect for GBP 60

4.22 Main stock solution stability of GBP (93 hrs at room temp.) 61

4.23 Main stock solution stability of LEV (93 hrs at room temp.) 62

4.24 Main stock solution stability of GBP (93 hrs at 2-8 °C) 62

1 2 3 4 5 6 7 8 9 10 11 12 13 ... 92 93

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